Optimizing Phosphorus Characterization in Animal Manures by Solution Phosphorus-31 Nuclear Magnetic Resonance Spectroscopy

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Optimizing phosphorus characterization in animal manures by solution phosphorus-31 nuclear magnetic resonance spectroscopy.

A procedure involving alkaline extraction and solution 31P nuclear magnetic resonance (NMR) spectroscopy was developed and optimized for the characterization of P in animal manures (broiler, swine, beef cattle). Inclusion of ethylenediaminetetraacetic acid (EDTA) in the alkaline extraction solution recovered between 82 and 97% of the total P from the three manures, which represented a significa...

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Comparison of phosphorus forms in wet and dried animal manures by solution phosphorus-31 nuclear magnetic resonance spectroscopy and enzymatic hydrolysis.

Both enzymatic hydrolysis and solution (31)P nuclear magnetic resonance (NMR) spectroscopy have been used to characterize P compounds in animal manures. In this study, we comparatively investigated P forms in 0.25 M NaOH/0.05 M EDTA extracts of dairy and poultry manures by the two methods. For the dairy manure, enzymatic hydrolysis revealed that the majority of extracted P was inorganic P (56%)...

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Identification of scyllo-Inositol Phosphates in Soil by Solution Phosphorus-31 Nuclear Magnetic Resonance Spectroscopy

A large proportion of the organic P in soils can occur as scylloinositol phosphates. These compounds are rarely detected elsewhere in nature and remain poorly understood, partly because conventional procedures for their determination are lengthy and erroneous. We report a straightforward procedure for the determination of scylloinositol phosphates in soil extracts using solution 31P nuclear mag...

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Phosphorus 31 Magnetic Resonance Spectroscopy Study

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Reducing Phosphorus in Animal Manures

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ژورنال

عنوان ژورنال: Journal of Environmental Quality

سال: 2004

ISSN: 0047-2425

DOI: 10.2134/jeq2004.7570